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AssociationConnectingElectronicsIndustriesProvidedbyIHSunderlicensewithIPC
NoreproductionornetworkingpermittedwithoutlicensefromIHS
IPC-9204
2017-February
GuidelineonFlexibilityandStretchabilityTestingforPrinted
Electronics
AninternationalstandarddevelopedbyIPC
AssociationConnectingElectronicsIndustries
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InMay1995theIPC’sTechnicalActivitiesExecutiveCommittee(TAEC)adoptedPrinciplesofStandardizationasaguidingprincipleofIPC’sstandardizationefforts.
StandardsShould:
ShowrelationshiptoDesignforManufacturability(DFM)andDesignfortheEnvironment(DFE)
Minimizetimetomarket
Containsimple(simplified)language
Justincludespecinformation
Focusonendproductperformance
Includeafeedbacksystemonuseandproblemsforfutureimprovement
StandardsShouldNot:
Inhibitinnovation
Increasetime-to-market
Keeppeopleout
Increasecycletime
Tellyouhowtomakesomething
Containanythingthatcannotbedefendedwithdata
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IPC-9204
GuidelineonFlexibilityandStretchabilityTestingforPrintedElectronics
DevelopedbythePrintedElectronicsTestMethodDevelopmentandValidationSubcommittee(D-65)ofthePrintedElectroncsCommittee(D-60)ofIPC
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Usersofthispublicationareencouragedtoparticipateinthedevelopmentoffuturerevisions.
Contact:
IPC
3000LakesideDrive,Suite105NBannockburn,Illinois
60015-1249
Tel847615.7100
Fax847615.7105
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February2017 IPC-9204
Acknowledgment
Anydocumentinvolvingacomplextechnologydrawsmaterialfromavastnumberofsourcesacrossmanycontinents.WhiletheprincipalmembersofthePrintedElectronicsTestMethodDevelopmentandValidationSubcommitte(D-65)ofthePrintedElectronicsCommittee(D-60)areshownbelow,itisnotpossibletoincludeallofthosewhoassistedintheevolu-tionofthisstandard.Toeachofthem,themembersofIPCextendtheirgratitude.
PrintedElectronicsCommittee PrintedElectronicTestMethod
DevelopmentandValidationSubcommittee
TechnicalLiaisonoftheIPCBoardofDirectors
Co-ChairsNeilBolding
MacDermidEnthoneElectronicsSolutions
DanielGamota
PrintovateTechnologies,Inc.
Co-ChairsWeifengLiu
FlextronicsInternational
NeilBoldingMacDermidEnthoneElectronicsSolutions
BobNeves
Microtek(Changzhou)Laboratories
PrintedElectronicTestMethodDevelopmentandValidationSubcommittee
LeonardB.Allison,EngineeredMaterialsSystems,Inc.
SaiAvuthu,JabilCircuit,Inc.LanceAuer,RaytheonCompanyAnirbanBasu
AndyBehr,PanasonicIndustrialDevicesSalesCompanyofAmerica(PIDSA)
NeilBolding,MacDermidEnthoneElectronicsSolutions
AlanM.Burk,ALMAXMarcCarter,SAIC
DonDupriest,LockheedMartinMissiles&FireControl
MahendraS.Gandhi,NorthropGrummanAerospaceSystems
KenGann,LabTech
MaryAliceGill,JabilCircuit,Inc.JoshGoldberg,TaiyoAmericaInc.
ScottE.Gordon,DuPontTeijinFilmsMaryK.Herndon,Raytheon
Company
MichaelJ.Jawitz,OrbitalATKKellyKovalovsky,i3ElectronicsMuradKurwa,GEHealthcareJeffreyLee,ISTGroup
JieLian,Flextronics
WeifengLiu,FlextronicsInternational
KarenMcConnell,NorthropGrummanCorporation
DeboraL.Obitz,NTS-BaltimoreJanObrzut,NIST
JeffreyParker,Insulectro
RavindranPeriasamy,SandiaNationalLabsAlbuquerque
BenjaminPiepgrass,SouthwestResearchInstitute
CassandraRocha,BoeingCompanyHaridossSarma,GO2Scout4R&TPaulShaw,In2Tec
RussellS.Shepherd,.NationalTechnicalSystemsAnaheim
JeffShubrooks,RaytheonCompanyRichardC.Snogren,BristleconeLLCBrianJ.Toleno,Microsoft
Corporation
LouisY.Ungar,AdvancedTestEngineeringSolutions,Inc.
SteveJ.Vetter,NSWCCraneMichaelJ.Watson,BluestarSiliconesDianeH.Williams,Corning
Incorporated
MobinYahyazadehfar,DuPontEngineeringPolymers
SpecialAcknowledgment
LeonardB.Allison,EngineeredMaterialsSystems,Inc.
NeilBolding,MacDermidEnthoneElectronicsSolutions
AlanM.Burk,ALMAX
DonDupriest,LockheedMartinMissiles&FireControl
KenGann,LabTech
MaryAliceGill,JabilCircuit,Inc.WeifengLiu,Flextronics
International
KarenMcConnell,NorthropGrummanCorporation
MobinYahyazadehfar,DuPontEngineeringPolymers
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iii
ProvidedbyIHSunderlicensewithIPC
NoreproductionornetworkingpermittedwithoutlicensefromIHS
IPC-9204 February2017
ThisPageIntentionallyLeftBlank
AssociationCoivnnectingElectronicsIndustries
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February2017 IPC-9204
TableofContents
SCOPE 1
Purpose 1
APPLICABLEDOCUMENTS 1
IPC 1
ASTM 1
InternationalElectrotechnical
Commission(IEC) 2
InternationalOrganizationforStandardization(ISO) 2
TERMSANDDEFINITIONS 2
Bending 2
Crease 2
Crumple 2
Curing 2
Flexibility 2
FlexographyPrinting 2
GravurePrinting 2
InkJetPrinting 2
MinimumBendingRadius 2
Preconditioning 2
PrintedElectronics 2
PrintedElectronicsProcess 2
ScreenPrinting 3
Stretchability 3
StretchablePrintedElectronics 3
Torsion 3
WearablePrintedElectronics 3
WearableSmartDevices 3
TESTPREPARATIONANDSETUP 3
TestSpecimenPreparationandStorage 3
SpecimenPreconditioning 3
StandardTestConditions 3
TestEquipment 3
TestSetupandParameters 3
Monitoring 3
Inspection 4
SUMMARYOFPRINTEDELECTRONICSFLEXIBILITYANDSTRETCHABILITYTESTS 4
STRETCHABILITYTESTINGPRINCIPLES 5
StretchabilityLimitTest 5
CyclicStretchabilityTest 5
StretchabilityUnderConstantElongationConditions 6
StretchabilityUnderConstantTorsion
Conditions 6
StretchabilityUnderCyclicTorsionConditions 7
BENDINGTESTPRINCIPLES 7
VariableRadiusBendingTest 7
VariableAngleBendingTest 8
FreeArcBendingTest 9
DeMattiaFlexibilityTest 9
LoopBendingTest 10
FoldingEnduranceTest 10
TORSIONTESTPRINCIPLES 11
ROLLINGTESTPRINCIPLES 12
RollingFlexTest 12
CoilingFlexTest 13
SlidingPlateTest 13
CRUMPLINGTESTPRINCIPLES 14
CreaseTest 14
SchildknechtFlexTest 15
CrumpleFlexTest 16
VampFlexTest 17
BallyFlexTest 17
APPENDIXATESTREPORT
RECOMMENDATIONS 18
APPENDIXBSTANDARDREFERENCES 19
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IPC-9204 February2017
Figures
Figure6-1 StretchabilityTestingofPrintedInk 5
Figure7-1 VariableRadiusBendingTestSetup 7
Figure7-2 VariableAngleBendingTestSetup 8
Figure7-3 FreeArcBendingTestSetup. 9
Figure7-4 DeMattiaFlexTestSetup 9
Figure7-5 LoopBendingTestSetup 10
Figure7-6 TestSetupUsingMITFoldingEndurance
TestInstrument 10
Figure8-1 TorsionTestSetup 11
Figure9-1 RollingFlexTestSetup 12
Figure9-2 CoilingFlexTestSetup 13
Figure9-3 SlidingPlateTestSetup. 13
Figure10-1 CreaseFlexTestSetup 14
Figure10-2 SchildknechtFlexTestSetup 15
Figure10-3 CrumpleFlexTestSetup 16
Figure10-4 BallyFlexTestSetup 17
Tables
Table5-1 PrintedElectronicsFlexibilityand
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StretchabilityTests 4
TableA-1 TestReportRecommendations 18
AssociationvCionnectingElectronicsIndustries
February2017 IPC-9204
GuidelineonFlexibilityandStretchabilityTestingforPrintedElectronics
SCOPE
Thisguidelinedescribesflexibilityandstretchabilityteststhatmaybeusedtoevaluateprintedelectronicsforflexible,stretchableandwearableapplications.
PurposeThisguidelinedescribestestswhichtheIPCD-65PrintedElectronicsTestMethodsandValidationSubcom-mitteedeemedappropriateforconsiderationforflexibilityandstretchabilitytestingofprintableelectronics.ThedescriptionsofthesetestswereprovidedbymembersoftheD-65Subcommittee.
Thisguidelinedoesnotrepresentanendorsementofanyofthedescribedtests.Itisintendedonlyasaneducationalresource,especiallyforthesmarttextilesandwearableprintedelectronicsmarkets,untilstandardizedtestmethodsaredevelopedandapproved.
TheD-65Subcommitteeinvitesusers,suppliers,testlaboratoriesandotherinterestedpartiestosubmitadditionaltestsormodificationstothoseexplainedhereinfornextrevisionsofthisguideline.
Thisguidelinealsoincludesreferencestoindustry-approvedtestmethodswhichcanbeusedoradaptedforflexibilityandstretchabilitytestingforprintedelectronics(seeSection5andAppendixB).
APPLICABLEDOCUMENTS
Thedocumentslistedinthissectionarethosewhicharereferencedinthebodyofthisguideline.AppendixBalsoprovidesacompendiumofindustry-approvedtestmethodswhichmaybeadaptedforflexibilityandstretchabilitytestingofprintedelectronics.
IPC1
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IPC-T-50TermsandDefinitionsforInterconnectingandPackagingElectronicCircuits
IPC-TM-650TestMethodsManual
IPC-6903TermsandDefinitionsfortheDesignandManufactureofPrintedElectronics
ASTM2
ASTMF392StandardPracticeforConditioningFlexibleBarrierMaterialsforFlexDurability
ASTMD430StandardTestMethodsforRubberDeterioration—DynamicFatigue
ASTMD813StandardTestMethodforRubberDeterioration—CrackGrowth
ASTMF2749StandardTestMethodforDeterminingtheEffectsofCreasingaMembraneSwitchorPrintedElectronicDevice
ASTMF2750StandardTestMethodforDeterminingtheEffectsofBendingaMembraneSwitchorPrintedElectronicDevice
ASTMD6182StandardTestMethodforFlexibilityandAdhesionofFinishonLeather
AssociationConnectingElectronicsIndustries 1
IPC-9204 February2017
InternationalElectrotechnicalCommission(IEC)3
IEC62715-6-1Flexibledisplaydevices-Part6-1:Mechanicalstresstestmethods
IEC62899-201Printedelectronics-Part201:Materials-Substrates
InternationalOrganizationforStandardization(ISO)4
ISO5402-2Leather—Determinationofflexresistance—Part2:Vampflexmethod
ISO5626Paper—Determinationoffoldingendurance
ISO7854Rubber-orplastics-coatedfabrics—Determinationofresistancetodamagebyflexing
TERMSANDDEFINITIONS
Inadditiontothetermsanddefinitionslistedhere,thereaderisreferredtoIPC-6903foradditionaltermsonflexiblehybridprintedelectronicsandprintedelectronicsandtoIPC-T-50fortermsonPCBsandPCBassemblies.
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BendingDeformationofprintedelectronicscausedbyexternalstressperpendiculartotheflatplaneofspecimen.
CreaseTomakealine,ridgeorgrooveonaprintedelectronicdevicewhichusesasubstratesuchasclothorpaperbyaddingpressuretofoldthesubstrateordevice.
CrumpleTocrushaprintedelectronicdevicewhichusesasubstratesuchasclothorpapersothatitformsnonuni-formfolds.
CuringAprocessduringwhichvolatilecomponents,ifpresent,evaporateandmaterialsundergochemicalreactionstoformacontinuousbulkmaterial.
FlexibilityThepropensityofaprintedelectronicdevicetobebent,creasedorstretched.
FlexographyPrintingAprintingprocesswhichusesaflexiblepositivemaster(flexoplate)totransferamediumfromasourcetoatargetsubstrateviapressureusingananiloxroller.
GravurePrintingPrintingmethodinwhichanimageisappliedtoaprintingsubstratebyuseofamasterimagecar-rierandthenthereverseoftheimagetobetransferredisengravedandetched.
InkJetPrintingAtypeofnoncontactprintingmethodthatrecreatesadigitalimagebypropellingdropletsofinkontopaper,plasticorothersubstrates.
MinimumBendingRadiusThesmallestbendingradiusatwhichaspecimendoesnotbreakordoesnotshowperma-nentdamage.
PreconditioningAsetofconditionsexposedonthetestspecimenpriortoactualtestingthateithersimulatetherealuseconditionsorbringthetestspecimentotherequiredstate.
PrintedElectronicsDevicesmanufacturedusingprintedelectronicsprocesses.
PrintedElectronicsProcessAdditiveprintingmethodsusedtogenerateelectricalandelectroniccircuitryordevicesonavarietyofsubstrates.
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AssociationCo2nnectingElectronicsIndustries
February2017 IPC-9204
ScreenPrintingMethodofforcingmaterials(inkorpaste)throughapreparedscreen(eitherpolyesterorstainlesssteel)tocreateadesignpattern.
StretchabilityMechanicalpropertyofasubjecttorestoretoitsoriginalstateafterreleaseofatensionstresswhichpullsthesubjecttoacertainelongation.
StretchablePrintedElectronicsAprintedelectronicspartorproductthat,duetothedesignandtheintrinsicprop-ertiesofthematerialsandelementsusedtoconstructit,canbesubjectedtostaticanddynamicstrainwithoutanobserva-tioninperformancedegradation.Thesupplieroftheprintedelectronicprovidesguidanceastothepredefinedstrainlevelwherebytheassemblywillmaintainatleastaminimumlevelofperformance.
TorsionTheactionoftwistingasubjectbytheexertionofforces,tendingtoturnoneendorpartaboutalongitudi-nalaxiswhiletheotherisheldfastorturnedintheoppositedirection.
WearablePrintedElectronicsAprintedelectronicpartorproductthatcanbeattachedtoaperson’sbody(e.g.,arms,wrists,legs,waist,head,ear,etc.).Avarietyofstructuralelementsmaybeusedtoattachtheseproducts,suchasbutnotlimitedtoanelastomericmaterial(band),whichisamechanismthatintegratesadevicetoconstraintheassemblytoanarm,wristorleg(e.g.,Velcro,buckle,compressionfitting).Additionally,theycanbeaffixedtoaperson’sbodyviabiocom-patibleadhesivematerials.
WearableSmartDevicesWearableprintedelectronicswithafunctionalitytoconnectandinteractwithotherdevices,networks,theinternet,etc.
TESTPREPARATIONANDSETUP
TestSpecimenPreparationandStorageClearlydescribethetestspecimeninthetestreport.Thedescriptionshouldincludesamplesize,shapeanddimensions,materialsandstack-up,specialtreatmentpriortotesting,applicablestandardforspecimenpreparationand/orotherrelevantinformation.
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Specifythespecimenstorageconditionspriortotesting.Itisrecommendedtostorespecimensatatemperatureof20°Cto25°Candhumidityof30%to60%foratleast48hoursafterfabricationpriortotesting.Thiscanbedoneinacontrolledenvironment.Iftherearespecialrequirements,storageconditionsmaybedeterminedbetweenuserandsupplier.
SpecimenPreconditioningThespecimenmaybesubjectedtopreconditioningpriortostretchabilityandflexibilitytests,suchastemperatureaging,temperaturecycling,hightemperaturewithhumidity,durability,etc.,asagreeduponbetweenuserandsupplier.
StandardTestConditionsSpecifythetestconditionsintermsofatmosphere,temperatureandhumidity.Itisrecom-mendedtotestthespecimensat23°C±1°Cwitharelativehumidity(RH)50%±5%atambientatmosphereunlessotherwisespecified.Thespecimenmaybetestedatelevatedtemperatureorhumidityconditionsasagreeduponbetweenuserandsupplier.
TestEquipmentStatetheequipmenttobeusedinthetest,themakerofthemachineanditscapability.Gaugerepro-ducibilityandrepeatability(gaugeR&R)maybeperformedtoqualifytheequipmentandtestprocesspriortostretch-abilityandflexibilitytesting.AtestreportongaugeR&Rmaybeattachedtothefinaltestreport.
TestSetupandParametersClearlydescribethetestsetupinthetestreport(e.g.,fixturedesign,howthespecimenistobemountedonthefixture,etc.).Clearlydescribethetestparametersinthetestreport,suchassequence,strainrate,frequency,speed,lowerandupperlimitsofdisplacement,numberofcycles,etc.
MonitoringDescribehowthefunctionalityorelectricalresistanceoftestspecimensismonitoredduringthestretch-abilityandflexibilitytesting.Monitoringmaybedoneinsituorperiodicallyduring,priortoandaftertesting.Clearlystatedatatype,collectionfrequencyandacceptanceorrejectioncriteria.
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IPC-9204 February2017
InspectionInspectthespecimensbeforeandafterstretchabilityandflexibilitytests.Thismaybedonebyvisualinspection,opticalmicroscope,scanningelectronmicroscope(SEM)orotherinspectionequipment.Recordanyqualityabnormality,damages,failuresymptomsandlocations.Ifafailureoccurs,failureanalysismaybedonetoidentifytherootcausesofthefailure.
SUMMARYOFPRINTEDELECTRONICSFLEXIBILITYANDSTRETCHABILITYTESTS
Printedelectronicswillexperienceavarietyofflexibilitystressesintheirapplications.Accordingly,differenttestproceduresarebeingdevelopedtoevaluatethesestresses.Ingeneral,thetestscanbeclassifiedintofivebasiccategories:
Stretchability
Bending
Torsion
Rolling
Crumpling
Acombinationofthesetestswillgiverisetomoretestoptions.Thedeterminationofthetesttobeused,sequencesandtestparametersarebetweenuserandsupplier.
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Table5-1PrintedElectronicsFlexibilityandStretchabilityTests
Category
TestItems
ExemplaryApplications
ApplicableStandard
Stretchabilitytesting
Stretchabilitylimittest
Stretchableprintedink
Noknownindustrystandard
Cyclicstretchabilitytest
Stretchableprintedink
Noknownindustrystandard
Stretchabilityunderconstantelongationcondition
Stretchableprintedink
Noknownindustrystandard
Stretchabilityunderconstanttorsioncondition
Stretchableprintedink
Noknownindustrystandard
Stretchabilityundercyclictorsioncondition
Stretchableprintedink
Noknownindustrystandard
Bendingtest
Variableradiusbendingtest
Flexibledisplay
IEC62715-6-1
Variableanglebendingtest
Flexiblebattery
Noknownindustrystandard
Freearcbendingtest
Flexibledisplay,flexibleOLEDlighting
Noknownindustrystandard
DeMattiaflexibilitytest
Wearableelectroluminescentlighting
ASTMD813,ASTMD430,ISO7854
Loopbendingtest
Wearablekeyboard
Noknownindustrystandard
Foldingendurancetest
Wearablewristband
ISO5626,IEC62899-201
Torsiontest
Torsiontest
Flexibleelectroluminescentdisplay
Noknownindustrystandard
Rollingtest
Rollingflextest
Rolltorollprinting,e-paper
ASTMF2750
Coilingflextest
Rolltorollprinting,e-paper
Noknownindustrystandard
Slidingplatetest
Flexibledisplay,flexiblebattery
Noknownindustrystandard
Crumplingtest
Creasetest
Printedinkcircuit
ASTMF2749
Schildknechtflextest
Wearablegarment
ISO7854
Crumpleflextest
Wearablegarment
ISO7854,ASTMF392
Vampflextest
Wearablegarmentandfootwear
ISO5402-2
Ballyflextest
Wearablegarmentandfootwear
ASTMD6182
AssociationCo4nnectingElectronicsIndustries
February2017 IPC-9204
STRETCHABILITYTESTINGPRINCIPLES
A
B
C
D
E
A IPC-9204-6-1
Thetestsin6.1through6.5areexamplesofthosewhichcanbeusedtoevaluatethefunc-tionalityofprintedelectronicdevicesunderrepeatedorconstantuniaxialstretchconditions.Theprinciplesdescribedinthissectioncanbeapplicabletobiaxialstretchabilitytestingaswell.
StretchabilityLimitTestThistestmethodcanbeusedtodeterminetheelongationlimit,inpercentage,ofprintedelectronicsbyuniaxialtensiletesting.Samplesmaybepre-paredintheoriginalproductformorusingtestcouponsuchasstraightedgestripsor‘‘dogbone’’stripsasdescribedinASTME-345,orotherformsagreeduponbetweenuserandsupplier.AschematictestsetupforevaluatingstretchabilityofprintedinkisshowninFig-ure6-1.
Thestretchablecircuitisheldfirmlybetweentwofixtures.Cushionsmaybeaddedattheinterfacebetweenthesamplegripsandconductiveinktopreventstressconcentrationandabnormalresistancereadings.Inthistest,thebottomfixturecanremainstationarywhilethetopfixtureismovable.Bymovingthefixture(s),thespecimenisstretchedtoacertainper-centageuntilthecircuitphysicallyorelectricallyfailsduringthestretchabilitytest.Itisimportanttocontinuouslymonitorthefunctionalityorresistanceofthecircuit.Intheothertestoptionbothfixturesaremovableandthespecimenisstretchedwhenthetwofixturesmoveinoppositedirections.
Note:
Stretchability%FinalinklengthInitialinklength
Initialinklength
TheinklengthmaybeobtainedbymeasuringthedistancebetweenthetwosamplegripsasshowninFigure6-1.Finalinklengthmaybedeterminedbypreviouslyestablishedfailurecriterionintermsofresistanceincreaseoftheprintedink,suchasmaximumvalueofresis-tance,resistanceincreasepercentage,etc.
Includethefollowinginthetestreport:
Descriptionofthespecimen
Samplesize
Environmentaltestconditions
Strainrate
Initiallength,displacementandforce
Stretchabilitylimit(inpercentage)
Failurecriteria
Continuouselectricaltestresults
Inspectionbeforeandaftertest
Plottheelectricaltestdataversusthestretchpercentage.
Figure6-1StretchabilityTestingofPrintedInk
A–Linktoresistancemeasurementprobe
B–Movingsampleholder
C–Stretchableink
D–Stretchablesubstrate
E–Stationarysampleholder
CyclicStretchabilityTestThistestmethodcanbeusedtoverifyifastretchable/wearableprintedelectronicdevicecanwithstandrepeatedelongationcyclesunderatensileload.SetupthetestasshowninFigure6-1,withthestretchablecircuitheldfirmlybetweentwofixtures.Inthistest,thebottomfixturecanremainstationary,whilethetopfixtureismov-ableorbothfixturescanmove.Bymovingthefixture(s)upanddown,thespecimenisstretchedtoacertainpercentageandthen,afteracertainholdingtime,returnstoitsinitialstatewhenloadisreleased.Thespecimenisstretchedagaintorepeatforsecondcycle.Continuouslymonitorthefunctionalityorresistanceofthecircuit.
Includethefollowinginthetestreport:
Descriptionofthespecimen
Samplesize
Environmentaltestconditions
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5
IPC-9204 February2017
Cyclicloadingprofileandfrequency
Strainrate
Initiallength,displacementandforce
Stretchpercentage
Holdingtime
Failurecriteria
Numberofcyclesperspecimen
Continuouselectricaltestresults
Inspectionbeforeandaftercycling
Plotelectricaltestdataversusthestretchpercentageandnumberofcycles.
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StretchabilityUnderConstantElongationConditionsThistestcanbeusedtoevaluatethefunctionalityoftheprintedelectronicdevicesunderconstantelongationconditions.AsshowninFigure6-1,thestretchablecircuitisheldfirmlybetweentwofixtures.Thebottomfixtureremainsstationary,whilethetopfixtureismovable.Bymovingthetopfixtureup,thespecimenisstretchedtoacertainpercentageandthenmaintainedatthesameelongationpercentageforaprolongedduration.Continuouslyorperiodicallymonitorthefunctionalityorresistanceofthecircuit.Includethefollowinginthetestreport:
Descriptionofthespecimen
Samplesize
Environmentaltestconditions
Strainrate
Initiallength,displacementandforce
S
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