ICS

97.195；19.020

CCS

Y04

中華人民共和國國家標準

GB/T44205—2024

古代漆膜顯微觀察樣品制備

Samplepreparationofancientlacquerfilmformicroscopy

2024-07-24發(fā)布2024-11-01實施

國家市場監(jiān)督管理總局發(fā)布

國家標準化管理委員會

GB/T44205—2024

目次

前言

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Ⅲ

1

范圍

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1

2

規(guī)范性引用文件

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1

3

術語和定義

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1

4

取樣

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1

4.1

取樣計劃

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1

4.2

取樣過程

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2

4.3

包裝與保存

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2

5

包埋

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2

5.1

包埋材料

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2

5.2

包埋模具

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2

5.3

樣品前處理

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2

5.4

樣品放置

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3

5.5

樣品包埋

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3

6

研磨

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3

7

拋光

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3

附錄A（資料性）

古代漆膜顯微觀察樣品取樣信息記錄表樣式

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4

參考文獻

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5

Ⅰ

GB/T44205—2024

前言

本文件按照GB/T1.1—2020《標準化工作導則第1部分：標準化文件的結構和起草規(guī)則》的規(guī)

定起草。

請注意本文件的某些內容可能涉及專利。本文件的發(fā)布機構不承擔識別專利的責任。

本文件由中華人民共和國國家文物局提出。

本文件由全國文物保護標準化技術委員會（SAC/TC289）歸口。

本文件起草單位：中國科學技術大學、中國國家博物館、福建理工大學、中國文化遺產研究院、北

京中科標準科技集團有限公司。

本文件主要起草人：龔鈺軒、龔德才、鐵付德、王志民、喬成全、周光昭、成維智、鐘博超、

于晨、張曉寧、王開、周霄、曾小凡。

Ⅲ

GB/T44205—2024

古代漆膜顯微觀察樣品制備

1范圍

本文件規(guī)定了古代漆膜顯微觀察樣品的取樣、包埋、研磨、拋光的制備要求。

本文件適用于反射光學顯微鏡和掃描電子顯微鏡觀察的古代漆膜顯微觀察樣品制備的操作。

2規(guī)范性引用文件

下列文件中的內容通過文中的規(guī)范性引用而構成本文件必不可少的條款。其中，注日期的引用文

件，僅該日期對應的版本適用于本文件；不注日期的引用文件，其最新版本（包括所有的修改單）適用

于本文件。

GB/T13298—2015金屬顯微組織檢驗方法

WW/T0003館藏出土竹木漆器類文物病害分類與圖示

3術語和定義

WW/T0003界定的以及下列術語和定義適用于本文件。

3.1

取樣sampling

用工具從文物本體或附屬于文物本體的殘件（片）上獲取樣品的操作。

3.2

包埋embedding

用樹脂材料包裹、固定待觀察樣品，便于后續(xù)處理和觀察的操作。

3.3

研磨grinding

用附著于合適襯底（如紙或布）上無取向分布的硬質顆粒打磨樣品表面的操作。

[來源：GB/T30067—2013，2.2.301]

3.4

拋光polishing

用介質與樣品之間的機械作用來消除研磨所造成的人為損傷粗糙面，得到一個光滑反射面的操作。

[來源：GB/T30067—2013，2.2.188，有修改]

4取樣

4.1取樣計劃

古代漆膜顯微觀察樣品（以下簡稱“樣品”）制備應根據取樣目的制定取樣計劃，取樣計劃的相關

要求如下：

a）取樣應有代表性，宜選取同時包含基體、漆灰層、漆膜層、顏料等區(qū)域的樣品；