資料文件1H最氘試（磁劑化位表碳原子

氘代四氫呋喃

氘代二氯甲烷

氘代氯仿

氘代甲

氘代苯

氘代氯

氘代丙

氘代DMSO

氘代乙1.72

5.32

7.26

2.08

7.16

6.96

2.05

2.5

1.94氘代試劑位移（溶劑峰）

3.58

6.977.01

6.997.147.09水峰乙酸丙酮乙腈苯正丁醇

OHaceticCH3CH3CHCH3

sacidssss

2.46CH32.051.957.311.15

1.52s2.121.977.351.24

1.561.892.172.17.361.28

0.432.061.570.697.121.03

0.42.11.550.587.151.05

1.031.571.771.217.21.12

2.84b1.522.092.057.361.18

3.33b1.762.092.077.371.11

2.131.962.081.967.371.16OH

sc

3.16

0.58

0.63

1.3

4.19

2.18氯仿

CH

s

7.89

7.32

7.26

6.1

6.15

6.74

8.02

8.32

7.5818-DMF

冠醚6

CH2CHCH3CH3

ssss

3.577.912.882.76

3.597.962.912.82

3.678.022.962.88

3.367.572.371.96

3.397.632.361.86

3.417.732.512.3

3.597.962.942.78

3.517.952.892.73

3.517.922.892.77二惡烷DME乙烷乙醇環(huán)己胺二氯乙烷二氯甲烷乙醚二甘醇二甲醚乙酸乙酯乙烯乙二醇六甲基苯正己烷

CH2CH3CH2CH3CH3CH2OHCH2CH2CH2CH3CH2CH2CH2OCH3CH3COCH2CH3CH2CH2CH3CH3CH2

sssst,7q,7dsc,ssst,7q,7mmssq,7t,7ssest,7m

3.563.283.430.851.13.513.31.443.775.511.123.383.433.533.281.944.041.195.363.482.180.891.29

3.653.343.490.851.193.661.331.443.765.331.153.433.573.53.3324.081.235.43.662.20.891.27

3.713.43.550.871.253.721.321.433.735.31.213.483.653.573.392.054.121.265.43.762.240.881.26

3.333.123.310.810.973.360.831.42.914.321.13.253.433.313.121.693.870.945.253.362.10.881.22

3.353.123.330.80.963.340.51.42.94.271.113.263.463.343.111.653.890.925.253.412.130.891.24

3.453.173.370.791.063.511.391.373.264.771.13.313.493.373.161.783.961.045.293.582.10.851.19

3.593.283.460.831.123.573.391.433.875.631.113.413.563.473.281.974.051.25.383.282.170.881.28

3.573.243.430.821.063.444.631.43.95.761.093.383.513.383.241.994.031.175.413.342.140.861.25

3.63.283.450.851.123.542.471.443.815.441.123.423.533.453.291.974.061.25.413.512.190.891.281/3

資料文件吡啶吡咯吡咯啉硅脂四氫呋喃甲苯

CH(2,6)CH(3,5)CH(4)NHCH(2,5)CH(3,4)CH2(2,5)CH2(3,4)CH3CH2(2,5)CH2(3,4)CH3

mmmbrmmmmsmms

8.547.257.65t6.666.022.751.590.113.621.792.31

8.597.287.689.966.796.192.821.670.093.691.822.34

8.627.297.688.696.836.262.871.680.073.761.852.36

8.476.676.998.46.436.272.541.360.263.541.432.11

8.536.666.987.716.486.372.541.330.293.571.42.11

8.516.97.257.86.626.272.641.430.143.591.552.16

8.587.357.768.616.776.070.133.631.792.32

8.587.397.7910.026.736.012.671.55-0.063.61.762.3

8.577.337.7310.756.756.12.751.610.083.641.82.33CH(2,4,6)

m

7.1

7.15

7.17

6.96-7.01

7.02

7.01-7.087.10-7.20

7.18

7.10-7.30CH(3,5)

m

7.19

7.24

7.25

7.09

7.13

7.10-7.177.10-7.20

7.18

7.10-7.30三乙胺六甲基二硅醚HMPAc咪唑甲烷甲醇

CH3CH2CH3CH3H2CH4CH3

tqsdsss

0.972.460.072.584.550.193.27

0.992.480.072.64.590.213.42

1.032.530.072.654.620.223.49

0.952.390.12.424.50.173.03

0.962.40.122.44.470.163.07

0.932.390.12.474.490.153.25

0.962.450.072.594.540.173.31

0.932.43a0.062.534.610.23.16

0.962.450.072.574.570.23.28OH

S

3.02

1.09

1.09

1.3

3.12

4.01

2.16硝基甲烷正戊烷丙烷2-丙丙烯吡啶

CH3CH3CH2CH3CH2CH3CHCH3CH2(1)CH2(2)CHCH(2,6)CH(3,5)CH(4)

stmtseptdseptdtdmdmmmmm

4.310.891.310.91.331.083.821.694.894.995.798.547.257.65

4.310.891.30.91.321.173.971.714.935.035.848.597.287.68

4.330.881.270.91.321.224.041.734.945.035.838.627.297.68

3.010.871.250.891.320.953.651.554.924.985.78.476.676.99

2.940.871.230.861.260.953.671.554.955.015.728.536.666.98

3.590.841.230.841.261.043.821.584.914.985.728.516.97.25

4.430.881.270.881.311.13.91.684.955.818.587.357.76

4.420.861.270.871.291.043.781.684.945.035.88.587.397.79

4.310.891.290.91.331.093.871.74.935.045.858.577.337.7313C代試（核試）化位移碳原子

氘代四呋喃

氘代二甲烷

氘代氯

氘代甲

氘代苯

氘代氯

氘代丙

氘代DM67.21

53.84

77.16

137.48

128.06

134.19

29.84

39.5225.31

128.87

129.26

206.26氘代試劑位移（溶劑峰）

127.96125.1320.43

128.25125.962/3

資料文件乙酸

171.69

175.85

175.99

175.3

175.82

175.67

172.31

171.9

20.13

20.91

20.81

20.27

20.37

20.51

20.95丙酮

204.19

206.78

207.07

204

204.43

204.83

205.87

206.3

30.17

31

30.92

30.03

30.14

30.12

30.56乙腈

CN

116.79

116.92

116.43

115.76

116.02

115.9